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of transforming waste materials into clean hydrogen fuel using high-temperature steam and air. Oxidative pyrolysis of cellulose containing moisture was examined in the CMHR in order to determine the presence of air, oxygen, and moisture during the pyrolysis process. A test sample containing 75% cellulose and 25% moisture by weight was pyrolyzed in a gaseous environment that contained 1.428 mol of air for each mole of cellulose. Numerical calculations were performed according to: C6 H10 O5 + 3H2 O + 0.3(O2 + 3.76N2 ) = = Products = The results show a reduction in CO and unburned hydrocarbon concentration and a corresponding increase in CO2 production with the addition of air and moisture, as compared to the pure pyrolysis case. The calculated results showed similar trends; see Figure 15.6. The amount of pyrolyzed gases generated as well as their composition and heating value are important for the design and development of waste destruction systems and to control the emission of pollutants. Signi cant increase in both the heating value and volume of gases produced during cellulose pyrolysis can be seen with an increase in pyrolysis temperature; see Figure 15.7. At temperatures below 3000 K, large amounts of H2 and CH4 are found. At temperatures greater than 3000 K there is a sharp increase in the H species (atomic hydrogen) and C species (carbon gas) formation due to the thermal decomposition of CH4 , CO2 , CO, and other higher molecular weight gases; see Table 15.6. In addition, it is also to be noted that no solid char residue remains at such high temperatures. 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However, these differ from quantitative UV/Vis techniques in their greater spectral complexity, narrower absorption bands, and the technical limitations of IR instruments. Quantitative determinations obtained from IR spectra are usually inferior in quality and robustness to those obtained with UV/Vis and NIR spectroscopy. In addition, univariate or linear cali- (3.22) CEnter/CLose/Direction/Halfwidth/Line/Radius/Second pt/Undo/Width]: These circuit parameters were used in Kennedy [9], and the phase portrait in Fig. 10.21 is essentially that in Fig. 5 of that article [9]. The MATLAB code that generates Fig. 10.21 appears in Appendix 10.B. For the parameters in (10.154) the circuit simulation phase portrait in Fig. 10.21 is that of a strange attractor [11, 16], and so is strongly indicative (although not conclusive) of chaotic dynamics in the circuit. 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